Multiple-pulse techniques for solid-state nuclear magnetic resonance spectroscopy of materials / Anthony D. Montina

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dc.contributor.authorMontina, Tony
dc.contributor.authorUniversity of Lethbridge. Faculty of Arts and Science
dc.contributor.supervisorHazendonk, Paul
dc.date.accessioned2012-02-23T23:10:13Z
dc.date.available2012-02-23T23:10:13Z
dc.date.issued2010
dc.degree.levelMasters
dc.descriptionxviii, 179 leaves ; 29 cmen_US
dc.description.abstractSolid state NMR has the ability to obtain detailed structural information at the molecular level in materials. This has led to the development of a large number of high resolution techniques, some of which utilize multiple pulse methods. The behaviour of these multiple pulse techniques has, to date, been explained using either relaxation or spin dynamics. Ultimately, an explanation based on a combination of both dynamics is required in order to properly understand the underlying mechanism of these techniques. This work presents an explanation of the experimental behaviour observed for three multiple pulse domain selection techniques: the DIVAM, Direct DIVAM, and Refocused DIVAM sequences. This is based on a combination of spin and relaxation dynamics and is accomplished using both analytical expressions and simulations obtained using a general simulation program for solid-state NMR spectroscopy (SIMPSON).en_US
dc.identifier.urihttps://hdl.handle.net/10133/2614
dc.language.isoen_USen_US
dc.publisherLethbridge, Alta. : University of Lethbridge, Dept. of Chemistry and Biochemistry, c2010en_US
dc.publisher.departmentDepartment of Chemistry and Biochemistryen_US
dc.publisher.facultyArts and Scienceen_US
dc.relation.ispartofseriesThesis (University of Lethbridge. Faculty of Arts and Science)en_US
dc.subjectNuclear magnetic resonance spectroscopyen_US
dc.subjectSolid state chemistryen_US
dc.subjectDissertations, Academicen_US
dc.titleMultiple-pulse techniques for solid-state nuclear magnetic resonance spectroscopy of materials / Anthony D. Montinaen_US
dc.typeThesisen_US
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